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An abstract of the dissertation of Nicolas Noel Hamel for the Doctor of Philosophy in Environmental Sciences and Resources: Chemistry presented on January 20, 1995. Title: Monomeric and Polymeric Fluoroalkyl Sulfonyl Fluorides, Sulfonate Salts and Sulfonic Acids for Use as Electrolytes and coatings Monomeric and pOlymeric fluoroalkyl sulfonyl fluorides, sulfonate salts and sulfonic acids have qualities desirable for use as electrolytes in alternative energy sources such as fuel cells and solid polymer electrolyte lithium batteries. Since the nature of the fluoroalkyl group affects the properties of these compounds, new monomeric and polymeric fluoroalkyl sUlfonyl fluorides, sulfonate salts and sulfonic acids were prepared in this work. Simple compounds prepared in this work were: the fluoroalkyl sUlfonyl fluorides, sulfonate salts and sulfonic acid CHF (OCF2CF2S02F) 2' CF2(OCF2CF2S02F) 2' CH2(OCF2CF2S03Na) 2' CF2(OCF2CF2S03 ) 2Ca , CF2(OCF2CF2S03H) 2' prepared by means of electrochemical fluorination; FC (CF3 ) 20CH2CH20CF2CF2S02F prepared using the adduct of hexafluoroacetone and silver fluoride; CH30CF2CF2S02F prepared

Monomeric and Polymeric Fluoroalkyl Sulfonyl Fluorides, Sulfonate Salts and Sulfonic Acids for Use as Electrolytes and Coatings