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Abstract A high-throughput experimental (HTE) approach starting from dry, fine-grained powders was used to synthesize bulk samples in the system (K x Na 1− x ) 1− y Li y (Nb 1− z Ta z )O 3 , a doped variant of the piezoelectric (K 0.5 Na 0.5 )NbO 3 (KNN). Starting from the system (K 0.5 Na 0.5 ) 1− y Li y (Nb 1− z Ta z )O 3 known from the works of Saito et al. an effort was made to establish a higher order phase diagram. Special emphasis was put on expanding the known morphotropic phase boundary that constitutes a region of special interest for electroceramic materials as it features maximum piezoelectric properties. Analyses were performed using a HTE-compatible technique, namely automated powder X-ray diffraction (XRD).

Investigation of phase boundaries in the system (KxNa1-x)1-yLiy(Nb1-zTaz)O3 using High-Throughput Experimentation (HTE)