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We show how to determine polybrominated diphenyl ethers in aqueous samples using liquid-liquid extraction and gas chromatography with electron capture detection (LLE-GC-μECD). This method, due to its simplicity, low limits of determination (7-9 pg/L), high accuracy, relatively low costs, and high recovery coefficients for all of these PBDEs (86-92%), offers enormous benefits for routine analyses of PBDEs. The developed method was applied to surface water samples collected from different sampling points in western Pomerania.

Determining Polybrominated Diphenyl Ethers in Surface Waters of Western Pomerania Using Gas Chromatography with Electron Capture Detection