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The non-isothermal decomposition of NiC 2 O 4 ·2H 2 O was investigated under a dynamic inert atmosphere using a temperature-programmed X-ray diffractometer (TP-XRD) and a thermogravimetric analyzer coupled to a Fourier-transform infrared spectrometer (TGA-FTIR). Both solid and gaseous products were analyzed in situ. The XRD pattern of the dehydration product did not match data for NiC 2 O 4  reported in the JCPDS file. The thermal decomposition of the dehydration product (NiC 2 O 4 ) took place in two sub-steps, both of which involved CO 2  evolution. Metallic nickel was the final product.

The Thermal Decomposition of NiC 2 O 4 ·2H 2 O: An In situ TP-XRD and TGA/FT-IR Study