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Powder samples of  β -Ni(OH) 2  and doped variants of the  α -Ni(OH) 2  structure type were prepared by a coprecipitation method. Chemical composition was analysed by ICP. Samples were measured by X-ray powder diffraction (XRD). Single peak profiles were analysed by fitting a splitted Pearson VII funktion to the measured patterns. Peak profile data were collected and a strong anisotropic peak broadening was observed. Structure models of possible stacking orders in  β -Ni(OH) 2  and doped  α -Ni(OH) 2  were developed. DIFFaX simulations of structure models with statistical stacking orders were carried out. The simulated peak profiles were compared to the measured ones and a fairly good agreement was found. A semiquantitative analysis of the stacking faults in these materials is shown.

Structural study of β -Ni(OH) 2 and α -Ni(OH) 2 variants for electrode applications