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[Ba 2 (C 2 H 6 O 2 ) 4 ][Ge 2 (C 2 H 4 O 2 ) 6 ] · 2.5 C 2 H 6 O 2  ( 3a ) is isolated from the reaction of GeO 2  · aq with Ba(OH) 2  · 8 H 2 O in glycol (1,2-ethanediol).  3a  crystallizes in the space group  P -1 with  a  = 10.324(2) Å,  b  = 13.932(3) Å,  c  = 15.800(3) Å,  α  = 102.86(2)°,  β  = 91.33°,  γ  = 109,47° and  V  = 2077.2(7) Å 3 . With increasing temperature  3a  looses glycol and forms step by step [Ba(C 2 H 6 O 2 ) 2 ][Ge(C 2 H 4 O 2 ) 3 ] ( 3b ), Ba[Ge(C 2 H 4 O 2 ) 3 ] ( 3c ) and finally hexagonal BaGeO 3  ( 4 ).

zeitschrift für kristallographie - crystalline materials

[Ba 2 (C 2 H 6 O 2 ) 4 ][Ge 2 (C 2 H 4 O 2 ) 6 ] · 2.5 C 2 H 6 O 2  – an ethanediolato complex of germanium. Synthesis, thermal decomposition and crystal structure