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ZrOI 2  · 8 H 2 O was synthesized from ZrI 4  and concentrated aqueous HI leading to colourless crystals. Single X-ray diffraction data gave a monoclinic cell with  a  = 8.392(5) Å,  b  = 37.497(5) Å,  c  = 16.217(5) Å and  β  = 102.76(6) Å in  P 2 1 / c . The zirconyl cation is tetrameric, the iodide anions exhibit no contacts to the zirconium atoms but are linked to the tetrameric cations by weak hydrogen bridge bonds.

Tetranuclear [Zr 4 (OH) 8 (H 2 O) 16 ] units in the crystal structure of ZrOI 2 · 8 H 2 O