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The stoichiometry of  1  was derived from the results of elemental analysis, IR,  1 H,  13 C-NMR, UV-Vis and mass spectroscopic techniques. The structure derived from physico-chemical methods is consistent with that of the X-ray diffraction. The compound crystallizes in the triclinic system, space group  P 1̅, with  a  = 9.3895(12),  b  = 11.3759(11),  c  = 12.8077(14)Å,  α  = 103.290(3)°  β  = 98.110(4)°,  γ  = 105.545(3)°,  V  = 1252.4(2)Å 3 ,  Z  = 2. The molecule has a non-planar configuration. The methoxy carbonylmethyl group exhibits an E-configuration. The crystal structure is stabilized by intermolecular C—H…O, N—H…O and O—H…O contacts.

zeitschrift für kristallographie - crystalline materials

Structure and characterization of methyl (±)-1-(2-aminophenyl)-2-hydroxy-4-(4-methoxybenzoyl)-5-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1 H -pyrrole-2-acetate