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The new complex oxide (V 0.5 Re 0.5 )O 2  has been synthesized under high pressure of 60 kbar at 1000°C, and its crystal structure determined by single crystal X-ray diffraction data analysis (S.G.:  P 4 2 / mnm ,  a  = 4.6357(4) Å,  c  = 2.8292(3) Å, V = 60.80(1) Å 3 ). This compound adopts a rutile-type structure with random cat ion distribution on one crystallographic site. The substitution of 50 vanadium by rhenium stabilizes the high temperature form of VO 2  at room temperature. The cation ratio of 1 : 1 was confirmed by EDX analysis performed by electron microscopy on the same crystals used for X-ray diffraction.

Preparation and crystal structure of a new high-pressure phase (V 0.5 Re 0.5 )O 2 with rutile-type structure