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The crystal and molecular structure of the title compounds have been determined by X-ray analysis ( N-(trichloroacetyl)morpholine , C 6 H 8 C l  3 NO 2 ,  P 2 1 / a ,  a  = 9.869(1) Å,  b  = 12.287(1) Å,  c  = 16.060(1) Å,  β  = 98.773(7)°,  Z  = 8;  2,6-di(trichloroacetyl)cyclohexanone , C 10 H 8 C l  6 O 3 ,  Pbca ,  a  = 10.553(1) Å,  b  = 15.405(2) Å,  c  = 18.435(2) Å,  Z  = 4). The morpholine and cyclohexane rings of both compounds adopt the chair conformation. There are some intra- and intermolecular hydrogen bonds in the title compounds, so the crystal structures of them are stabilized by C—H...Cl and C—H...O intra- and inter molecular hydrogen bonds.

Crystal structures of N-(trichloroacetyl)morpholine and 2,6-di(trichloroacetyl)cyclohexanone