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The structure of the organic derivative of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide, [C 32 H 28 N 2 O 5 ], has been determined by X-ray diffraction. The structure derived from the NMR spectroscopy, the IR spectra and elemental analysis is consistent with that of the X-ray diffraction. The compound crystalizes in the monoclinic system with space group  P 21/ c ,  a  = 16.234(1),  b  = 9.399(2),  c  = 19.389(1),  β  = 110.924(3)°,  V  = 2763.3(5) Å 3  and  Z  = 4. In the crystal, there is one weak C—H…O type intermolecular hydrogen bond interaction.

Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide