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Crystals of Cu(OH)F and Cu 3 (OH) 2 F 4  have been synthesized at low-hydrothermal conditions in sizes up to 0.3 mm. The structures were solved from CCD X-ray single-crystal data and refined to  R  = 0.033 and 0.019, respectively.

Crystal structures and Raman spectra of Cu(OH)F and Cu 3 (OH) 2 F 4