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The low-temperature boride Pd 5 B (Pd 16 B 3 ) formscongruently from the corresponding interstitial solid solu-tion Pd(B) (Pearson-Parthé symbol  cF (8-x), space group  Fm 3̅ m ) at 658 K. The structure of Pd 5 B has been investigated by X-ray powder diffraction yielding the following structural data:  I 4/ mmm ,  tI 2.38; unit cell parameters  a  = 0.28490(4) nm,  c  = 0.40038(9) nm,  c / a  = 1.405 &lt; √2, with the occupation 2Pd ( a ) and 0.19 x 2B ( b ). The crystal chemical data of Pd 5 B and some other homeotypic interstitial compounds of transition metals have been compared.

The structure of the palladium-rich boride Pd 5 B (Pd 16 B 3 )