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High quality nonstochiometric Tb- and Gdbased single crystals Tb 0.81 Ca 0.19 F 2.81  (TCF), Tb 0.76 Sr 0.24 F 2.76  (TSF), Gd 0.85 Ca 0.15 F 2.85  (GCF), Gd 0.83 Sr 0.17 F 2.83  (GSF) are analyzed in crystallographic detail by single-crystal X-ray diffraction measurements. TSF shows only main reflections, and its structure is refined to a disordered P6 3 /mmc structural model. Additional satellite reflections observed in GSF lead to an ordered twinned P3̅

Analysis of disordered nonstoichiometric Ln 1–x Ae x F 3–x (Ln = Tb or Gd, and Ae = Ca or Sr) single crystals