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At ambient conditions (NO) 2 SnCl 6  is isostructural with the corresponding titanium and vanadium salts which all crystallize in space group  P 4/ mnc  ( Z  = 2) and display a fourfold disorder of the NO +  ions. Below  T  c  = 229 K the diffraction pattern splits into the components of a quadruplet twin, but unlike for (NO) 2 VCl 6  remarkable discontinuities of the lattice parameters are not observed.

The crystal structure of the low-temperature phase of (NO) 2 SnCl 6 and ordering of the NO + ions