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A rare-topology [Mn II  4 ]-core complex [Mn 4 Br 4 (ppko) 4 (CH 3 OH) 4 ] ( 1 ; ppkoH = phenyl 2-pyridyl ketoxime) was synthesized  via  a solvothermal route and characterized by X-ray diffraction, IR, EPR, ESI-MS and magnetic properties measurements. In  1  Mn 2+  ions are bridged with phenyl 2-pyridyl ketoxime ligands. Bromine atoms and methanol molecules are terminal ligands. A comparison is made to the reported analogues with different terminal ligands pattern.

Structure and properties of a rare-topology [Mn II 4 ]-core complex with terminal bromido ligands