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Crystals of sarcosine sarcosinium nitrate (2 Sar · HNO 3 ) have been grown and characterized at 296 and 150 K by single crystal XRD and vibrational spectroscopy. The species was found to be triclinic (space group  P -1,  a  = 5.320(1) Å,  b  = 6.578(1) Å,  c  = 15.957(2) Å,  α  = 95.448(6)°,  β  = 95.944(6)°,  γ  = 93.410(6)°,  V  = 551.6(1) Å 3 , and  Z  = 2 at 296 K), with a dimeric sarcosine ... sarcosinium cation and a nitrate anion in the asymmetric unit. A very strong hydrogen bond connects the molecules within the dimer. In addition, the tensor of thermal expansion was determined for the temperature range of 200 to 290 K. A strong anisotropy was detected, with thermal expansion along the  c -axis approximately 14 times as strong as along the  a -axis.

Crystal structure at 296 and 150 K, vibrational spectra and thermal behaviour of sarcosine sarcosinium nitrate