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The crystal structure of (TMA) 2 [TiF 6 ] between –173 °C and 180 °C was refined on the basis of single crystal diffraction data. A phase transition from rhombohedral to cubic at approx. 142 °C was found by measuring the birefringence as a function of temperature, and confirmed by the refined crystal structures.

zeitschrift für kristallographie

Temperature dependent lattice distortion and high temperature phase transition of pseudo-cubic bis(tetramethylammonium) hexafluorotitanate (IV), (TMA) 2 [TiF 6 ]