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The crystal structures of two new compounds were determined: 4-ethyl-3-(4-methyl-1,2,3-thiadiazol-5-yl)- s -triazole-5-thione ( 1 ),  P 2 1 / n ,  a  = 10.433(2),  b  = 7.975(2),  c  = 13.100(3) Å,  β  = 110.70(3)° and 4-carboxymethyl-3-(4-methyl-1,2,3-thiadiazol-5-yl)- s -triazole-5-thione ( 2 ),  P 2 1 / c ,  a  = 6.444(1),  b  = 14.721(3),  c  = 11.067(2) Å,  β  = 93.50(3)°. In both structures, the molecules form ähydrogen-bonded dimers through N1—H1n···S1 (triaäzole···S=C-triazole) interactions. The crystal structure of  1  is further stabilized by intermolecular C—H···N and S···S interactions, while in  2 , C—H···N/O, O—H···N/S, S···S/O and π···π interactions are observed.

zeitschrift für kristallographie

Synthesis and crystal structure of 4-ethyl-3-(4-methyl-1,2,3-thiadiazol-5-yl)- s -triazole-5-thione and 4-carboxymethyl-3-(4-methyl-1,2,3-thiadiazol-5-yl)- s -triazole-5-thione