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The synthesis, characterization, and X-ray crystal structure of two new compounds were determined:  N -butyl-5-(4-methyl-1,2,3-thiadiazol-5-yl)-1,3,4-thiadiazol-2-amine ( 1 ) crystallizes in the monoclinic space group  P 2 1 / n  with  a  = 5.222(1),  b  = 15.010(3),  c  = 15.343(3) Å,  β  = 93.30(3)°,  Z  = 4 and 5-isoquinolin-3-yl- N -(2-methylphenyl)-1,3,4-thiadiazol-2-amine ( 2 ) crystallizes in the monoclinic space group  P 2 1 / c  with  a  = 7.455(2),  b  = 17.113(5),  c  = 12.199(3) Å,  β  = 94.68(2)°,  Z  = 4. In both structures, intermolecular N—H···N hydrogen bonds link two neighbouring molecules into a centrosymmetric R 2  2 (8) dimer.

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Synthesis and crystal structure of  N -butyl-5-(4-methyl-1,2,3-thiadiazol-5-yl)-1,3,4-thiadiazol-2-amine and 5-isoquinolin-3-yl- N -(2-methylphenyl)-1,3,4-thiadiazol-2-amine