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Crystal structures of five tin(IV) complexes containing the tetrahydrothiophene-1-oxide ligand, C 4 H 8 SO, TMSO, with Sn—O interactions, are described. They are trigonal bipyramidal Ph 2 SnCl 2 (TMSO), with TMSO and Cl in axial sites, and the octahedral complexes, Ph 2 SnCl 2 (TMSO) 2  and SnX 4 (TMSO) 2 , where  X  = Br or Cl. In the octahedral complexes, the TMSO ligands are  cis  to one another and are  trans  to the halides. The SnCl 4 (TMSO) 2  complex has been obtained in two crystalline forms, one orthorhombic and isostructural with SnBr 4 (TMSO) 2 , and the other triclinic. Strengths of the interactions of the tin halides with dimethyl sulfoxide, (DMSO), and TMSO ligands are compared.

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Tetrahydrothiophene-1-oxide, TMSO, complexes of tin(IV) halides: crystal structures of SnCl 4 (TMSO) 2 [two polymorphs], SnBr 4 (TMSO) 2  and Ph 2 SnCl 2 (TMSO) n  ( n  = 1 and 2)