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NH 4 [NiGa 1.84 In 0.16 (PO 4 ) 3 (H 2 O) 2 ] orthophos phate was prepared through hydrothermal synthesis and analyzed by means of single crystal X-ray diffractometry. It was solved within  C 2/ c  monoclinic space group;  a  = 13.2483(8) Å,  b  = 10.2468(8) Å,  c  = 8.9033(7) Å,  β  = 108.637(1)°,  V  = 1145.27(15) Å 3 . Phosphorous atoms display tetrahedral arrangement, occupying two distinct sites; Ni atoms form NiO 4 (OH 2 ) 2  distorted octahedra, while Ga and In atoms share the same site forming (Ga,In)O 5  units with trigonal bipyramidal geometry. (Ga,In)O 5 , NiO 4 (OH 2 ) 2  and PO 4  units are linked together through edge- and vertex-sharing arrangements, making up the three-dimensional framework, completed by (NH 4 ) +  counter-ions. Strong O—H…O and N—H…O hydrogen bonds contribute to stabilize the array: O—H…O interactions were also investigated by means of Libowitzky formula (Libowitzky, 1999) application, owing to the results of IR spectroscopy.

Indium-doped gallophosphate NH 4 [NiGa 1.84 In 0.16 (PO 4 ) 3 (H 2 O) 2 ]: synthesis, X-ray crystal structure and IR spectroscopy