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In this study we report the solution of the structure of  δ -Al(OD) 3 . The crystal structure was determined using powder X-ray diffraction and direct methods, while the positions of deuterium atoms were estimated by difference-Fourier methods and MEM/Rietveld analysis. In the A-site deficient hydroxy-perovskite-type structure of  δ -Al(OD) 3 , we find two types of one-dimensional H-bonding network.

zeitschrift für kristallographie

Crystal structures of high-pressure phases in the alumina-water system: II. Powder X-ray diffraction study of a new dense aluminum deuteroxide,  δ -Al(OD) 3