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The crystal and molecular structure of the red brown form of [Fe 2 (η 5 -C 5 H 4 Me) 2 (CO)(CN)(μ-CO) · (μ-CNMe 2 )] has been determined by X-ray crystallography. It crystallises with one molecule per asymmetric unit ( P 2 1 / c ) and CO/CN disorder among the terminal ligands. It is a  cis  isomer with a non-planar Fe 2 (μ-C) 2  bridge having a dihedral angle of 154° between the two Fe 2 C planes. The Fe—C distances to the 2-electron donor ligands (CO, CN, μ-CO and μ-CNMe 2  + ) can be rationalised on the basis of their σ donor and π acceptor abilities.

The structure of the red-brown form of [Fe 2 (η 5 -C 5 H 4 Me) 2 (CO)(CN)(μ-CO)(μ-CNMe 2 )] and its confirmation as a cis isomer