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The crystal structutes of Cd(ReO 4 ) 2  · 4Urea, Cd(ReO 4 ) 2  · 6Urea and Ca(ReO 4 ) 2  · 5Urea were solved. Cd(ReO 4 ) 2  · 4Urea consists of discrete neutral [Cd(ReO 4 ) 2 L 4 ] (L = Urea) clusters. Ca(ReO 4 ) 2  · 5Urea and Cd(ReO 4 ) 2  · 6Urea are built up of cationic [Ca(ReO 4 )L 5 ]+ and [CdL 6 ]2+ clusters, respectively, and ReO 4 - anions, interlinked by an extensive network of H-bonds. The octahedral coordination of M atoms is most regular in Cd(ReO 4 ) 2  · 6Urea and most distorted in Ca(ReO 4 ) 2  · 5Urea.

zeitschrift für kristallographie - crystalline materials

Crystal structures of Cd(ReO 4 ) 2  · 4Urea, Cd(ReO 4 ) 2  · 6Urea and Ca(ReO 4 ) 2  · 5Urea. Synthesis and characterization of urea adducts from the systems M(ReO4) 2 -Urea-H 2 O, M = Ca, Sr, Ba, Pb and Cd