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Li 10 Zn 4 O 9  was synthesized by solid state reaction of the binary oxides. Li 10 Zn 4 O 9  crystallizes tetragonal ( P 4 2 / nmc ,  a  = 972.63(3) pm,  c  = 465.01(2) pm,  V  = 439.91(3) · 10 6  pm 3 ,  Z  = 2, conventional  R  = 6.34%). Crystals of Li 10 Zn 4 O 9  always contain additional small amounts of Li 6 ZnO 4  as intergrowths, and show a complex systematic twinning. Li 10 Zn 4 O 9  crystallizes as an ordered defect-variant of the Li 2 O-structure (anti-CaF 2  type) with the oxygen anions forming a slightly distorted cubic close packing with the Li + -ions and the Zn 2+ -ions occupying tetrahedral sites in an ordered manner. The vacant tetrahedral sites establish defect-clusters with the Zn 2+ -ions. The twinning is determined by the structural relationship to the Li 2 O-structure.

Li 1 Zn 4 O 9 ,eine neue Defektvariante der Fluβspatstruktur – Verzwilligung und systematische Verwachsung mit Li 6 Zn0 4