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The bicyclic sulfamidite (C 17 H 17 NO 2 S) ( P 2 1 2 1 2 1 ,  a  = 9.735(3) Å,  b  = 16.27(1)Å,  c  = 9.467(6) Å,  Z  = 4,  R  = 0.037), shows a  R  configuration of the S atom, deduced from the known absolute  S  configuration of the asymmetric carbon in the starting prolinol derivative. This is also deduced from proton  1 H NMR. The molecules form intramolecular C–H … O bonds.

Crystal structure of the bicyclic sulfamidite: (2 R ,5 S )-(−)-4,4-diphenyl-1-aza-2-thia-3-oxabicyclo[3.3.0]octane-2-oxide