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Single crystals of H 4 [Mo(CN) 8 ] · 2 O(C 2 H 5 ) 2  · CH 3 OH · 2 H 2 O have been obtained by adding diethylether to a solution of H 4 [Mo(CN) 8 ] in methanol. The needle shaped crystals are triclinic with space group  P [unk] and lattice constants  a  = 1073.2(1) pm,  b  = 1119.1(1) pm,  c  = 1199.1(1) pm,  α  = 84.41(1)°,  β  = 78.28(2)°,  γ  = 76.38(2)°. The molybdenum atom has a distorted square antiprismatic environment of eight cyanide ligands. The substance itself can be considered as a coordination polymer with a double N–H–N linkage incorporating hydrogen bonded oxonium ions as well as methanol and diethylether molecules.

zeitschrift für kristallographie - crystalline materials

Crystal structure of tetrahydrogen-octacyanomolybdate-diethylether-methanol-water (1/2/1/2) H 4 [Mo(CN) 8 ] · 2 O(C 2 H 5 ) 2  · CH 3 OH · 2 H 2 O: A coordination polymer with double N–H–N linkage