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The crystal structure of bis{(di- i -butyldithiophosphinato)gold(I)}, {AuS 2 P( i -C 4 H 9 ) 2 } 2 , has been determined at 223 K. The white needles are triclinic, space group  P [unk], with unit-cell dimensions of  a  = 8.0238(5) Å,  b  = 8.9747(6) Å,  c  = 9.99655(7) Å,  α  = 64.965(1)°,  β  = 79.732(1)°,  γ  = 73.263(1)°,  Z  = 2, and  D  x  = 2.172 g/cm 3 . The structure was solved using direct methods and refined by a full-matrix least-squares procedure to a final  R ( F ) = 0.0278 and  Rw ( F  2 ) = 0.0638 using 2787 reflections. Bis{(di- i -butyldithiophosphinato)gold(I)} has a dimeric structure with bridging dithiophosphinate ligands and is essentially linear with an intramolecular Au···Au distance of 3.17 Å and no intermolecular interactions.

Crystal structure of bis{(di- i -butyldithiophosphinato)gold(I)}, {AuS 2 P( i -C 4 H 9 ) 2 } 2