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Single crystals of the new compound Li 2 Co 3 (SeO 3 ) 4  have been synthesized under low-hydrothermal conditions. The structure was determined by direct methods from single crystal X-ray diffraction data (monoclinic, space group  P 2 1 / c ,  a  = 8.095(2) Å,  b  = 9.236(3) Å,  c  = 7.781(2) Å,  β  = 115.76(1)°,  V  = 523.9 Å 3 ,  Z  = 2;  R 1 = 0.034 for 1613  F  o  &gt; 4 σ ( F  o ) and 98 variables). Li 2 Co 3 (SeO 3 ) 4  builds a framework structure composed of one type of [4 + 2] coordinated Li atoms and each two crystallographically different CoO 6  octahedra and pyramidal SeO 3  groups. The polyhedra of lithium and of one type of the cobalt atoms exhibit uncommonly strong irregular distortions.

Crystal structure, electronic absorption spectra, and crystal field superposition model analysis of Li 2 Co 3 (SeO 3 ) 4