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Single crystal neutron diffraction confirmed previously reported X-ray results: Co(Hdmg) 2 (NO 2 )(H 2 O) (Hdmg = dimethylglyoximate) crystallizes in the monoclinic space group  P 2 1 / m  with lattice constants  a  = 7.605(5) Å,  b  = 8.907(5) Å,  c  = 10.721 (5) Å,  β  = 94.07(3)°,  V  = 724.4(7) Å 3  and  Z  = 2 with the complex molecule on a mirror plane. In addition, the neutron diffraction experiment yielded accurate positions for all hydrogen atoms: The intramolecular hydrogen bridges O–H … O are asymmetric with distances O–H = 1.044(7) Å and O … H = 1.468(7) Å, and hence the chelating ligands are not equivalent. This intramolecular result correlates to the packing arrangement: The acceptor oxygen atom of the intramolecular bridge is also involved in strong intermolecular hydrogen bonding.

Crystal structure of aquabis(dimethylglyoximato)nitrocobalt(III) based on neutron diffraction data