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Powder samples of the system Sr 3− x  Ca  x  Al 2 O 6  ( x  = 0, 0.3, …, 2.7, 3.0) were prepared by means of solid state reactions at 1723 K. The lattice constants determined exhibit a linear dependence from the molar fraction  x  in the range 0.9 ≤  x  ≤ 3. For smaller values of  x  distinct deviations from this linearity are observed. As shown by the results of three single crystal investigations which could be carried out on crystals with  x  = 1.395(8), 1.62(1), and 2.12(1) this is due to a remarkable distribution of the earth alkaline metal atoms, which is far from being only statistical over the six crystallographically different sites.

zeitschrift für kristallographie - crystalline materials

Pulverdiffraktometrische Untersuchungen am System Sr 3− x  Ca  x  Al 2 O 6  sowie Einkristallstrukturanalysen für die Fälle  x  = 1,395(8), 1,62(1) und 2,12(1)