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The three Tl(I)-arsenates(V) Tl 3 AsO 4 ) [ a  = 8.517(3) Å,  c  = 5.233(2) Å, space group  P 6 3 ,  Z  = 2], Tl 2 Cu(I)(AsO 4 ) [ a  = 6.000(3) Å, = 5.343(2) Å,  c  = 8.616(3) Å,  β  = 98.05(3)°, space group  P 2 1 ,  Z  = 2], and TlCu(II) 2 (AsO 4 )(AsO 3 OH) [ a  = 6.407(2) Å,  b  = 11.245(4) Å,  c  = 10.173(3) Å,  β  = 98.64(2)°], space group  P 2 1 / c ,  Z  = 4] have been synthesized under hydrothermal conditions. Their structures were determined from single crystal X-ray diffraction data.

Structure investigations of Tl(I)-arsenates(V): Tl 3 (AsO 4 ), Tl 2 Cu(I)(AsO 4 ) and TlCu(II) 2 (AsO 4 )(AsO 3 OH)