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2,10 Dichloro 6-(2,3 dimethylphenoxy) dibenzo [ d .  g ] [1,3.6,2] dioxathiaphosphocin 6-sulphide (C 20 H 15 Cl 2 O 3 PS) crystallizes in the triclinic system,  P [unk] with  a  = 7.845(3) Å,  b  = 11.720(2) Å,  c  = 11.871(2) Å,  a  = 88.5(2)°,  β  = 73.6(2)°,  γ  = 89.1(2)°,  V  = 1046.7(4) Å3,  Z  = 2,  D  c  = 1.489M gm −3 , (Mo K α  ) = 0.71069 Å,  F (000) = 480 and  T  = 293 K. The crystal structure was solved by direct methods and refined by full matrix least-squares method to a final  R  = 0.0345 for 2701 unique observed reflections [ I  ≥ 2 σ ( I )]. The chlorobenzene rings A &amp; B which are at 68.8° to each other, are oriented respectively at 19.9° and 61.6° to the phenyl ring and both are at 36.5° to the best plane of the heterocyclic ring. The heterocyclic ring adopts a distorted boat chair conformation.

Structure of 2,10 dichloro 6-(2,3 dimethylphenoxy) dibenzo [ d , g ] [1,3,6,2]dioxathiaphosphocin 6-sulphide