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We report about the crystal structure of Cu 12 P 20 Br 10 , a polyphosphide containing the new polyanionic phosphorus polymer [unk][P 20  2− ]. It crystallizes in the triclinic system, space group  P [unk] (No. 2) with  a  = 9.886(2) Å,  b  = 13.190(2) Å,  c  = 14.763 (3) Å,  α  = 70.83(1)°,  α  = 82.68(1)°,  γ  = 80.13(1)°,  V  = 1786.1 (6) Å 3  and  Z  = 2. The phosphorus atoms build up one dimensional negatively charged tubes consisting of condensed 5- and 6-membered rings. They are connected via copper atoms to form double tubes oriented parallel [010] and are embedded between wavy layers of copper and bromine atoms. All copper atoms except those that are linked to negatively charged P-atoms are strongly disordered.

Crystal structure of Cu 12 P 20 Br 10 , a polyphosphide containing a new phosphorus polymer