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The structure of the title compound, crystallized from benzene, in the monoclinic system, space group  P 2 1 / c , with  a  = 9.032(3) Å,  b  = 10.111(1) Å,  c  = 14.625(1) Å,  β  = 121.3(1)°,  Z  = 4, has been solved from diffraction data collected on 2D imaging plate detector. This method allowed successful integration of non-uniform reflection profiles with short exposure time. Structural results revealed correct reaction path in the synthesis.

Crystal structure of 4-acetyl-l-(4′-fluorophenyl)-5-methyl-2,3-dihydro-1 H -pyrrole-2,3-dione verifies the scheme of synthesis