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At room temperature bis(trimethylphenylammonium) tetrachlorozincate, C 18 H 28 Cl 4 Zn, crystallizes in the monoclinic space group,  C 2/ c ,  a  = 1555.4(2) pm,  b  = 955.6(2) pm,  c  = 3086.6(5) pm,  β  = 95.38(1)°,  Z  = 8. The asymmetric unit contains two independent cations and one tetrahedral [ZnCl 4 ] 2−  anion. The atoms of one cation occupy fixed positions in the crystal structure, the other cation shows disorder of the methyl groups. The X-ray data indicate that this disorder is caused by a dynamic rotation of the (CH 3 ) 3  N group. IR and Raman data are given at room temperature as well as the results of DSC measurements in the range from 190 K to 370 K.

The structure of [(CH 3 ) 3 (C 6 H 5 )N] 2 ZnCl 4 at room temperature