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YbFe 2 Al 10  crystallizes with a new structure type, which was determined from single-crystal X-ray data:  Cmcm ,  a  = 896.6(1)pm,  b  = 1015.3(2)pm,  c  = 900.3(1) pm,  Z  = 4,  R  = 0.024 for 795 structure factors and 41 variable parameters. The structure is closely related to the tetragonal ThMn 12  and CeMn 4 Al 8  type structures, from which it can be derived by substitution of some manganese by aluminum atoms, and in addition it has a different stacking of atomic layers. The ytterbium atoms have 20 neighbors (4 Fe + 16 Al), the iron atoms have distorted icosahedral coordination (2 Yb + 10 Al), and all of the five different aluminum sites are coordinated by ytterbium, iron, and aluminum atoms with coordination numbers 12, 13, and 14.

The crystal structure of YbFe 2 Al 10 , a combined substitution and stacking variant of the ThMn 12 and CeMn 4 Al 8 type structures