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In  N , N -dimethyldithiocarbamylacetonethiosemicarbazone, C 7 H 14 N 4 S 3  (triclinic,  P [unk],  a  = 6.226(1) Å,  b  = 8.111(1) Å,  c  = 12.387(1) Å,  α  = 85.19(2)°,  β  = 84.81(1)°,  γ  = 74.21(2)°), the sulfur atom of the = N–NH–C(=S)–NH 2  unit is hydrogen bonded to the amino nitrogen atom of an adjacent molecule to form a centrosymmetric dimer. Tris(hydroxymethyl)-methylammonium  N , N -dimethyldithiocarbamylacetate, C 9 H 20 N 2 O 5 S 2  (monoclinic,  P 2 1 / c ,  a  = 10.773(2) Å,  b  = 10.2615(8) Å,  c  = 13.116(3) Å,  β  = 109.253(9)°) adopts a 3- d  network structure in which the cation is linked to the sulfur and carboxyl atoms of adjacent anions by hydrogen bonds.

zeitschrift für kristallographie - crystalline materials

Crystal structures of  N , N -dimethyldithiocarbamylacetonethiosemicarbazone and tris(hydroxymethyl)methylammonium  N , N -dimethyl-dithiocarbamylacetate