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N , N ′-ethylene-bis(1-ethyl-5,5-dimethyltetramic acid-3-acetiminato)copper(II)/(I) crystallizes in space group  P 2 1 / c :  a  = 11.164(4) Å;  b  = 12.340(8) Å;  c  = 17.069(3) Å;  β  = 99.76(2)°;  V  = 2317.5 Å 3 ;  Z  = 4;  D  x  = 1.376 g · cm −3 ; Mo K α   = 0.71069 Å;  μ  = 9.76 cm −1 ;  F (000) = 1012;  T  = 293 K; Conventional  R  = 0.052;  R w   = 0.051 for 4864 observed reflections.

Novel aspects in structures of copper (II) Schiff base complexes