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Single crystals of the compound Na 2 (Mg 3.6  · Fe 2.4 )[(Ge 5.6 Fe 0.4 )O 18 ]O 2  have been grown from a Na 2 O–MoO 3 –V 2 O 5  flux. The compound crystallizes in the triclinic  P [unk] space group with  a  = 8.994 Å,  b  = 9.924 Å,  c  = 10.495 Å,  α  = 64.30°,  β  = 84.07°,  γ  = 65.87° and  Z  = 2. The refinement of its structure using single-crystal X-ray data shows that it is isostructural with the silicate minerals aenigmatite, Na 2 (Fe 5 Ti)(Si 6 O 18 )O 2 , and krinovite, Na 2 (Mg 4 Cr 2 )(Si 6 O 18 )O 2 .

Structure refinement of Na 2 (Mg, Fe) 6 [(Ge, Fe) 6 O 18 ]O 2 , a new aenigmatite-analog