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The crystal and molecular structure of the title compound (BPIS hereafter) has been determined from three-dimensional X-ray data, measured on a computer-controlled STOE AED 2 diffractometer. The structure is triclinic Space group  P [unk], with  a  = 8.325(6) Å,  b  = 11.809(6) Å,  c  = 13.618(7) Å,  α  = 105.06(4)°,  β  = 104.46(5)°,  γ  = 99.57(5)°,  V  = 1212.99 Å 3 , and  Z  = 2.

Crystal structure of biphenylenyliodonium[bis(phenylsulphonyl)] methylsulphonylmethylide, C 28 H 21 IO 6 S 3