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The new ternary phosphides SrNi 9 P 5  and BaNi 10 P 6  were synthesized by heating the elements at 900°–1100°C. Single crystal X-ray methods revealed that SrNi 9 P 5  is isotypic with BaNi 9 P 5  and crystallizes hexagonally [ P 6 3 / mmc ;  Z  = 2;  a  = 6.529(1) Å,  c  = 10.732(1) Å], whereas BaNi 10 P 6  forms a new structure with orthorhombic symmetry [ Cmca ,  Z  = 4;  a  = 6.449(1) Å,  b  = 16.191(1) Å,  c  = 8.784(1) Å]. The structures are best described as an arrangement of alkaline-earth metal atoms, which are surrounded by Ni 18 P 12 (SrNi 9 P 5 ) and Ni 14 P 12  cages (BaNi 10 P 6 ), respectively.

Ni x P 12 -Käfige – Die Kristallstrukturen der Verbindungen SrNi 9 P 5 ( x = 18) und BaNi 10 P 6 ( x = 14)