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α  2 -Sn,  β  2 -Sn and the solid-state transition of  α  2 -Sn to  β  2 -Sn observed in tin grown by reduction of aqueous solutions of SnCl 2  with Mg are investigated by transmission electron microscopy (TEM) with selected area electron diffraction, Mössbauer spectroscopy and X-ray diffraction. Some data on the structure of two tin dioxides grown as additional products during the reduction of SnCl 2  with Mg and Al are included. The low sensitivity of the X-ray diffraction studies towards the  α  2 -Sn and its derivates, and towards the unusual SnO 2  structures is also discussed.

zeitschrift für kristallographie - crystalline materials

Electrochemically obtained tin – Part I: TEM, Mössbauer and X-ray investigations of  α  2 -Sn,  β  2 -Sn and some oxides grown during the reduction of SnCl 2