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The compounds PbMo 6 X 14  with X = Cl(I), Br(II), I(III) were synthesized from corresponding mixtures of lead(II) and molybdenum(II) halides. The crystal structures were determined by X-ray analyses and were refined in the cubic spacegroup  Pn [unk] (no. 201, sec. setting). The cell dimensions are I:  a  = 12.921(1) Å, II:  a  = 13.504(2) Å and III:  a  = 14.429(2) Å. The structures described below are isotypic to HgMo 6 Cl 14  although some differences are observed. Structural and crystal chemical relations will be discussed.

Darstellung und Kristallstruktur der homologen Reihe PbMo 6 X 14 , X = Cl, Br, I