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Al(O,F) 2  crystallizes as a high temperature reaction product of fine granined Al-oxides and a PbF 2 -melt. The space group is that of rutile (TiO 2 ),  P 4 2 / mnm  with unit cell dimensions  a  = 4.627 Å,  c  = 3.005 Å and  Z  = 2. The structure refinement based on 64 independent reflections and full-matrix least-squares method yielded  R  = 0.0195 ( R w   = 0.0102). The Alanion distances are 1.982(1) Å (equatorial) and 1.980(1) Å (apical), where the distortion of the anion-octahedron is reflected by the three different anion-anion-distances 2.579(2) Å (common edge), 2.802(2) Å, 3.005(2) Å and the equitorial angles (O,F) – Al – (O,F) within the octahedron are 81.3° and 98.7° respectively.

The rutile structure of Al 1− x □ x O 1−3 x F 1+3 x , x = 0.0886