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The molecular and crystal structure of the compound Bis-[1H-indole-3-ethylene-3′-methoxy-salicylaldimine]copper(II) monohydrate has been determined. This compound crystallizes in the monoclinic system,  C 2/ c  space group,  Z  = 4, cell dimensions  a  = 18.657(2),  b  = 7.194(1),  c  = 23.932(1) Å,  β  = 91.92(2)°,  V  = 3210(1) Å 3 ,  D  x  = 1.41 Mg/m 3 ,  F (000) = 1396. The structure has been refined to  R  = 0.043 and  wR  = 0.045 for 3643 independent observed reflections. The structure consists of one molecule of [C 18 H 17 N 2 O 2 ] 2 Cu and a water molecule not-coordinated to metal. The geometry around the copper atom is planar with the metal lying on a centre of symmetry. The water molecule plays an important role in the formation of  inter  molecular hydrogen bonding (OW … N(2) 2.900(9) and OW … O(21) (− x  + 1, − y , − z ) 2.848(3) Å).

Crystal structure and bonding of bis-(1H-indole-3-ethylene-3′-methoxy-salicylaldimine)copper(II) monohydrate