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We describe the synthesis and crystallisation by means of chemical vapour transport reactions of TiPO 4  and VPO 4 . TiPO 4  ( a  = 5.2985(5) Å,  b  = 7.911(1) Å,  c  = 6.3473(5) Å) and VPO 4  ( a  = 5.2316(5) Å,  b  = 7.7738(7) Å,  c  = 6.2847(5) Å) adopt the crystal structure of chromiumvanadate CrVO 4  ( Cmcm ,  Z  = 4). The results of the refinements of both crystal structures from single crystal data are given. TiPO 4  (VPO 4 ): 335 (223) symmetry independent reflections from 1260 (1439) reflections, 22 (22) variables, residuals.  R  = 0.062 (0.049).

Beiträge zum thermischen Verhalten wasserfreier Phosphate: VI.* Einkristallstrukturverfeinerung der Metall(III)-orthophosphate TiPO 4 und VPO 4