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The title compound is orthorhombic, with space group  B 2 mb  and  Z  = 4. The cell dimensions are  a  = 8.66036(1) Å,  b  = 14.51489(5) Å and  c  = 13.25635(6) Å. A total of 1626 independent reflections were measured with a SYNTEX P2 1  automatic diffractometer using Mo Kα  radiation. The structure was refined by a full-matrix least-squares procedure to a conventional  R  = 0.055 for the 1556 unique reflections. The co-ordination around the central copper atom is octahedral with the copper atom 0.78(4) Å above the equatorial plane of the four nitrogen atoms of the ligand molecule. The Cu – N equatorial plane bond lengths are 1.975 and 2.031 Å. The remaining positions of the co-ordination octahedron are occupied by a fluorine atom of one of the fluorophosphate groups and an oxygen of a water molecule. The Cu – F and Cu – O bond lengths are 2.7371 Å and 2.3968 Å respectively.

The crystal structure of bis[ethylenediamine]copper(II)fluorophosphatehydrate, Cu(en) 2 (PF 6 ) 2 · H 2 O