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The title compound, dimeric [Cu(bipy)(pht)] · 2H 2 O (CBP), has been synthesized by a simple new method and its crystal structure determined by X-ray analysis. The structure was solved by the heavy-atom method and by successive Fourier syntheses. CBP crystallizes in monoclinic space group  P 2 1 / n ,  a  = 15.685(11) Å,  b  = 12.900(9) Å,  c  = 8.825(3) Å,  β  = 100.45(3)°,  Z  = 4; 2983 unique reflections gave a final  R  = 0.057. The structure consists of centrosymmetric dimeric [Cu 2 (bipy) 2 (pht) 2 ] units together with the water of hydration. Water molecules are arranged in channels parallel to the  c -axis. The coordination geometry arround Cu is square pyramidal (the CuN 2 O 2 O′ chromophore).

The crystal and molecular structure of dimeric (2,2′-bipyridine)phthalatocopper(II) dihydrate